Karakterisasi Minyak Atsiri Daun Patikala (Etlingera elatior (Jack) R.m Smith) Metode Destilasi Air dengan GC-MS
Characterization of Essential Oil from Patikala Leaves (Etlingera elatior (Jack) R.m Smith) by Water Distillation Method with GC-MS
DOI:
https://doi.org/10.25026/jsk.v8i1.2597Abstract
Patikala (Etlingera elatior (Jack) R.M.Smith) is one type of plant from the Zingiberaceae family. Patikala leaves contain bioactive compounds such as polyphenols, alkaloids, flavonoids, steroids, saponins, and essential oils. Patikala leaf essential oil has the potential to be an antimicrobial and antioxidant agent. This research aims to characterize the essential oil from patikala leaves. The extraction method used water distillation and was characterized using GC-MS. The research results showed that the characteristics of essential oil obtained by water distillation method included a yield of 0.03%, organoleptic examination had a characteristic odor, was clear yellow in color, and contained active compounds such as Trans-3-caren-2-ol, p-Cymene, 1,3-Cyclopentadiene, dan 2-Cyclopenten-1-one. Based on the research, monoterpenoid essential oil was obtained.
Keywords: Essential oil, Etlingera elatior (Jack) R.M.Smith, Water distillation
Abstrak
Patikala (Etlingera elatior (Jack) R.M.Smith) merupakan salah satu jenis tanaman dari suku Zingiberazeae. Daun patikala mengandung senyawa bioaktif seperti polifenol, alkaloid, flavonoid, steroid, saponin dan minyak atsiri. Minyak atsiri daun patikala berpotensi sebagai agen antimokroba dan antioksidan. Penelitian ini bertujuan untuk karakterisasi minyak atsiri daun patikala. Metode ekstraksi menggunakan destilasi air dan dikarakterisasi menggunakan GC-MS. Hasil penelitian yang didapatkan karakteristik minyak atsiri metode destilasi air meliputi % rendamen untuk metode sebesar 0,03%, pemeriksaan organoleptik memiliki bau khas, berwarna kuning bening dengan kandungan senyawa aktif yaitu Trans-3-caren-2-ol, p-Cymene, 1,3-Cyclopentadiene, dan 2-Cyclopenten-1-one. Berdasarkan penelitian diperoleh minyak atsiri monoterpenoid.
Kata Kunci: Minyak atsiri, daun patikala, destilasi air
References
[1] W. Pipatrattanaseree, T. Thaptimthong, N. Boonrasri, S. Rattanajarasroj, S. Ontong, dan S. Chaisomboonpan, “Potential in vitro Anti-inflammatory and Anti-oxidant Activities of Various Extracts of Etlingera elatior Inflorescences.,” Asian Medical Journal and Alternative Medicine, vol. 23, no. 3, hlm. 64–71, Des 2023. https://asianmedjam.com/index.php/amjam/article/view/1443
[2] A. Khairunnisa, R. Yuniarti, G. I. Dalimunthe, dan Z. Rani, “Karakterisasi, Skrining dan Uji Aktivitas Antibakteri Ekstrak Etanol Bunga Kecombrang (Etlingera elatior (Jack) R.M.Sm) terhadap Staphylococcus aureus,” Journal of Pharmaceutical And Sciences, vol. 8, no. 2, hlm. 1033–1046, 2025, doi: 10.36490/journal-jps.com.v8i2.870.
[3] Y. P. Utami, R. Yulianty, Y. Y. Djabir, dan G. Alam, “Antioksidan Ekstrak Daun Patikala (Etlingera elatior (Jack) R.M. Sm) Penangkal Radikal Bebas ABTS Asal Enrekang Sulawesi Selatan,” JURNAL KATALISATOR, vol. 8, no. 2, hlm. 291–300, Nov 2023, doi: 10.22216/katalisator.v8i2.2572.
[4] E. Puspitasari, C. D. Pratiwi, D. R. Novian, dan D. D. R. Turista, “Antibacterial actifity of kecombrang (Etlingera elatior) leaf ethanol extract to against Klebsiella pneumoniae,” Edubiotik?: Jurnal Pendidikan, Biologi dan Terapan, vol. 7, no. 01, hlm. 36–42, 2022, doi: 10.33503/ebio.v7i01.1663.
[5] M. Sobhy dkk., “Essential oils as antibacterials against multidrug-resistant foodborne pathogens: Mechanisms, recent advances, and legal considerations,” Food Bioscience, vol. 64, hlm. 105937, Feb 2025, doi: 10.1016/j.fbio.2025.105937.
[6] R. C. e Silva dkk., “Monoterpenes and Sesquiterpenes of Essential Oils from Psidium Species and Their Biological Properties,” Molecules, vol. 26, no. 4, hlm. 965, Feb 2021, doi: 10.3390/molecules26040965.
[7] O. Yoo dan S.-A. Park, “Anxiety-Reducing Effects of Lavender Essential Oil Inhalation: A Systematic Review,” Healthcare (Basel), vol. 11, no. 22, hlm. 2978, Nov 2023, doi: 10.3390/healthcare11222978.
[8] C. Scandurra dkk., “The Effectiveness of Neroli Essential Oil in Relieving Anxiety and Perceived Pain in Women during Labor: A Randomized Controlled Trial,” Healthcare (Basel), vol. 10, no. 2, hlm. 366, Feb 2022, doi: 10.3390/healthcare10020366.
[9] J. Saikia dkk., “Effect of postharvest drying on physicochemical properties, volatile yield, composition, and sensory attributes of Alpinia zerumbet (shell ginger) rhizome,” Industrial Crops and Products, vol. 198, hlm. 116719, Agu 2023, doi: 10.1016/j.indcrop.2023.116719.
[10] K. Ashokkumar, J. Simal?Gandara, M. Murugan, M. K. Dhanya, dan A. Pandian, “Nutmeg ( Myristica fragrans Houtt.) essential oil: A review on its composition, biological, and pharmacological activities,” Phytother Res, vol. 36, no. 7, hlm. 2839–2851, Jul 2022, doi: 10.1002/ptr.7491.
[11] M. H. Raza dkk., “Comparative Study of Essential Oils Extracted From Foeniculum vulgare Miller Seeds Using Hydrodistillation, Steam Distillation, and Superheated Steam Distillation,” Food Sci Nutr, vol. 12, no. 12, hlm. 10535–10549, Des 2024, doi: 10.1002/fsn3.4593.
[12] Y. P. Utami, A. M. D. Kristiyanti, dan Imrawati, “Optimasi Waktu Penyulingan Terhadap Kadar dan Karakteristik Minyak Atsiri Daun Patikala(Etlingera elatior (Jack) R.M.Smith),” JURNAL KATALISATOR, vol. 7, no. 2, hlm. 205–212, Okt 2022, doi: 10.22216/katalisator.v7i2.979.
[13] Supriyadi, S., Handayani, S., dan Nugraha, P. (, “Pengaruh Variasi Metode Ekstraksi terhadap Rendemen dan Komponen Kimia Minyak Atsiri Daun Selasih.,” Jurnal Kimia Terapan Indonesia, vol. 25, no. 1, hlm. 58-64., 2023.
[14] S. Sangthong, I. Promputtha, P. Pintathong, dan P. Chaiwut, “Chemical Constituents, Antioxidant, Anti-Tyrosinase, Cytotoxicity, and Anti-Melanogenesis Activities of Etlingera elatior (Jack) Leaf Essential Oils,” Molecules, vol. 27, no. 11, Mei 2022, doi: 10.3390/molecules27113469.
[15] B. Mahdavi, W. A. Yaacob, dan L. B. Din, “Chemical composition, antioxidant, and antibacterial activity of essential oils from Etlingera sayapensis A.D. Poulsen & Ibrahim,” Asian Pacific Journal of Tropical Medicine, vol. 10, no. 8, hlm. 819–826, Agu 2017, doi: 10.1016/j.apjtm.2017.08.006.
[16] A. T. Hanke, P. D. E. M. Verhaert, L. A. M. van der Wielen, M. H. M. Eppink, E. J. A. X. van de Sandt, dan M. Ottens, “Fourier transform assisted deconvolution of skewed peaks in complex multi-dimensional chromatograms,” Journal of Chromatography A, vol. 1394, hlm. 54–61, Mei 2015, doi: 10.1016/j.chroma.2015.03.017.
[17] S. Syafri, I. Jaswir, F. Yusof, A. Rohman, M. Ahda, dan D. Hamidi, “The use of instrumental technique and chemometrics for essential oil authentication: A review,” Results in Chemistry, vol. 4, hlm. 100622, Jan 2022, doi: 10.1016/j.rechem.2022.100622.
[18] N. Koljan?i?, O. Vyviurska, dan I. Špánik, “Aroma Compounds in Essential Oils: Analyzing Chemical Composition Using Two-Dimensional Gas Chromatography–High Resolution Time-of-Flight Mass Spectrometry Combined with Chemometrics,” Plants (Basel), vol. 12, no. 12, hlm. 2362, Jun 2023, doi: 10.3390/plants12122362.
[19] S. A. Pachore, A. A. Shinde, dan L. sandip Gangadhar, “A Review On Chromatographic Separation Techniques,” vol. 02, no. 10, Okt 2024, doi: 10.5281/zenodo.13935296.
[20] Y. Wu, N. Zhang, K. Luo, Y. Liu, Z. Bai, dan S. Tang, “Recent advances of innovative and high-efficiency stationary phases for chromatographic separations,” TrAC Trends in Analytical Chemistry, vol. 153, hlm. 116647, Agu 2022, doi: 10.1016/j.trac.2022.116647.
[21] D. B. Hibbert, “Chemometric Analysis of Data from Essential Oils,” dalam Plant Volatile Analysis, H. F. Linskens dan J. F. Jackson, Ed., Berlin, Heidelberg: Springer, 1997, hlm. 119–140. doi: 10.1007/978-3-662-03331-9_6.
[22] S. Syafri, I. Jaswir, F. Yusof, A. Rohman, M. Ahda, dan D. Hamidi, “The use of instrumental technique and chemometrics for essential oil authentication: A review,” Results in Chemistry, vol. 4, hlm. 100622, Jan 2022, doi: 10.1016/j.rechem.2022.100622.
[23] F. M. Vella, R. Calandrelli, D. Cautela, I. Fiume, G. Pocsfalvi, dan B. Laratta, “Chemometric Screening of Fourteen Essential Oils for Their Composition and Biological Properties,” Molecules, vol. 25, no. 21, hlm. 5126, Nov 2020, doi: 10.3390/molecules25215126.
[24] G. Baccolo, B. Quintanilla-Casas, S. Vichi, D. Augustijn, dan R. Bro, “From untargeted chemical profiling to peak tables – A fully automated AI driven approach to untargeted GC-MS,” TrAC Trends in Analytical Chemistry, vol. 145, hlm. 116451, Des 2021, doi: 10.1016/j.trac.2021.116451.
[25] X. Fan dkk., “Fully automatic resolution of untargeted GC-MS data with deep learning assistance,” Talanta, vol. 244, hlm. 123415, Jul 2022, doi: 10.1016/j.talanta.2022.123415.
[26] Y. Tang dkk., “Profiling complex volatile components by HS-GC-MS and entropy minimization software: An example on Ligusticum chuanxiong Hort,” J Pharm Biomed Anal, vol. 218, hlm. 114854, Sep 2022, doi: 10.1016/j.jpba.2022.114854.
[27] M. Ivanovi?, K. Makoter, dan M. Islam?evi? Razboršek, “Comparative Study of Chemical Composition and Antioxidant Activity of Essential Oils and Crude Extracts of Four Characteristic Zingiberaceae Herbs,” Plants (Basel), vol. 10, no. 3, hlm. 501, Mar 2021, doi: 10.3390/plants10030501.
[28] M. B. Paji? dkk., “Influence of harvester type and harvesting time on quality of harvested chamomile,” Journal of Agricultural Sciences (Belgrade), vol. 61, no. 2, hlm. 201–213, 2016, doi: 10.2298/JAS1602201P.
[29] F. Les dkk., “Essential Oils of Two Subspecies of Satureja montana L. against Gastrointestinal Parasite Anisakis simplex and Acetylcholinesterase Inhibition,” Molecules, vol. 29, no. 19, hlm. 4640, Sep 2024, doi: 10.3390/molecules29194640.
[30] M. Habán, J. Korczyk-Szabó, S. ?erteková, dan K. Ražná, “Lavandula Species, Their Bioactive Phytochemicals, and Their Biosynthetic Regulation,” Int J Mol Sci, vol. 24, no. 10, hlm. 8831, Mei 2023, doi: 10.3390/ijms24108831.
[31] M. Firdaus dkk., “Peningkatan Rendemen Minyak Atsiri Melalui Maserasi Awal dengan Metode Ultrasonikasi di Rumah Atsiri Indonesia,” PRIMA: Journal of Community Empowering and Services, vol. 9, no. 1, hlm. 50–55, 2025.
[32] Harimurti, N, Soerawidjaja, T. H., Sumangat, D., dan Risfaheri. (, “Ekstraksi Minyak Nilam (Pogostemon Cablin Benth) Dengan Teknik Hidrodifusi Pada Tekanan,” Jurnal Penelitian dan Pengembangan Pertanian, vol. 41, no. 2, hlm. 119–128, 2022.
[33] Nurnasari, E., dan Prabowo, H., “Pengaruh Ukuran Sampel dan Lama Waktu Destilasi terhadap Rendemen Minyak Atsiri Tembakau Lokal Indonesia,” Prosiding Seminar Nasional Penelitian dan Pengabdian Masyarakat, hlm. 49–53, 2023.
[34] F. Siswantito dkk., “Produksi minyak atsiri melalui ragam metode ekstraksi dengan berbahan baku jahe,” Jurnal Inovasi Teknik Kimia, vol. 8, no. 3, hlm. 178–184, 2023.
[35] Kim, J. M., Lee, S. K., dan Park, H. Y., “Pharmacological effects of monoterpene alcohols derived from essential oils on the central nervous system: A mini-review,” Molecules, vol. 27, no. 18, hlm. 6016.
[36] Abebe, D., dan Getahun, T, “A review on the biological activities of p-Cymene and its potential applications in pharmaceuticals and food preservation. 13(1), 1-12.,” Journal of Applied Phytochemistry, vol. 13, no. 1, hlm. 1–12, 2024.
[37] Ramos-Silva, C, Dias, A., dan Oliveira, J. M., “Anti-inflammatory and antioxidant activities of monoterpenes and their structural analogs: A recent review.,” European Journal of Medicinal Chemistry, 2023.
[38] Patel, S. K. dan Singh, V. P., “Advances in Diels-Alder cycloaddition reactions involving cyclopentadiene and its derivatives.,” Tetrahedron Letters, 148, 154030., 2024.
[39] Shao, X., Zhang, T., dan Liu, Q., “Repellent and insecticidal activity of cyclic ketones from plant essential oils against stored-product pests.,” Pest Management Science, vol. 79, no. 6, hlm. 2351-2360., 2023.
[40] Guo, Y., Ma, Z., dan Chen, G, “Advanced applications of small molecular ketones in food flavouring and cosmetic industries.,” Food Chemistry, vol. 390, hlm. 133221., 2022.
[41] Puspita, E. R., Widyastuti, W., dan Yulianti, M. (, “Analisis Komposisi Kimia dan Parameter Mutu Minyak Atsiri Rimpang Kecombrang (Etlingera elatior) Berdasarkan Variasi Tempat Tumbuh.,” Jurnal Farmasi Indonesia, vol. 19, no. 2, hlm. 154–162, 2022.
[42] Hasanah, A., Utami, W., dan Pratiwi, D., “Karakteristik Mutu Minyak Atsiri Daun Kecombrang (Etlingera elatior) Hasil Destilasi Uap,” Jurnal Ilmiah Pendidikan dan Sains, vol. 2, no. 1, hlm. 7–14, 2022.
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